This third volume in the Developments in Paleoenvironmental Research series deals with the major terrestrial, algal, and siliceous indicators used in paleolimnology. Other volumes deal with the acquisition and archiving of lake sediment cores, chronological techniques, and large-scale basin analysis methods (Volume 1), physical and geochemical parameters and methods (Volume 2), zoological techniques (Volume 4), and statistical and data handling methods (Volume 5). These monographs will provide sufficient detail and breadth to be useful handbooks for both seasoned practitioners as well as newcomers to the area of paleolimnology. Although the chapters in these volumes target mainly lacustrine settings, many of the techniques described can also be readily applied to fluvial, glacial, marine, estuarine, and peatland environments.

Numerical and statistical methods have rapidly become part of a palaeolimnologist’s tool-kit. They are used to explore and summarise complex data, reconstruct past environmental variables from fossil assemblages, and test competing hypotheses about the causes of observed changes in lake biota through history. This book brings together a wide array of numerical and statistical techniques currently available for use in palaeolimnology and other branches of palaeoecology. ​ Visit http://extras.springer.com the Springer's Extras website to view data-sets, figures, software, and R scripts used or mentioned in this book.

This first volume in the Developments in Paleoenvironmental Research series deals with the acquisition and archiving of lake sediment cores, chronological techniques, and large-scale basin analysis methods used in paleolimnology. Other volumes deal with physical and geochemical parameters and methods (Volume 2), biological techniques (Volumes 3 and 4), and statistical and data handling methods (Volume 5). These monographs provide sufficient detail and breadth to be useful handbooks for both seasoned practitioners as well as newcomers to the area of paleolimnology. Although the chapters in these volumes target mainly lacustrine settings, many of the techniques described can also be readily applied to fluvial, glacial, marine, estuarine, and peatland environments.

Theory Instrumentation NIR analysis of sediment samples Uses of NIRS in palaeolimnology Future perspectives Summary References Fly-ash particles. Neil Rose 319 12. Introduction A brief history Methods of extraction and enumeration Temporal distribution Spatial distribution Source apportionment The future Summary Acknowledgements References Part III: Stable Isotope Techniques 13. Application of stable isotope techniques to inorganic and biogenic carbonates. Emi Ito 351 Introduction Nomenclature and systematics of lake-water Mg/Ca and Sr/Ca ratios of lake-water of dissolved inorganic carbon (DIC) Carbonates in lake-sediments Mollusks Ostracodes Charaphytes Isotope analysis Preparation of carbonate samples for isotope analysis Conclusions Summary Acknowledgments References 14. Carbon and oxygen isotope analysis of lake sediment cellulose: methods and applications. Brent B. Wolfe, Thomas W. D. Edwards, Richard J. Elgood & Kristina R. M. Beuning 373 xi Introduction Stable isotope tracers in lake Historical development Methods Key criteria for paleohydrologic reconstruction Applications Future research directions Summary Acknowledgements References Nitrogen isotopes in palaeolimnology. Michael R. Talbot 15. 401 Introduction Nitrogen in lakes: forms and distribution Nitrogen isotopes Nitrogen isotope studies in palaeolimnology: sampling and measurement Some examples Closing remarks Summary Acknowledgments References Glossary, acronyms and abbreviations 441 Index 493 xiii PREFACE The explosive growth of paleolimnology over the past two decades has provided impetus for the publication of this series of monographs detailing the numerous advances and new techniques being applied to the interpretation of lake histories. This is the second volume in the series and deals mainly with physical and geochemical analytical techniques.

Volume package: Tracking Environmental Change Using Lake Sediments. Volumes 1-5

Paleolimnology is a rapidly developing science that is now being used to study a suite of environmental and ecological problems. This volume is the fourth handbook in the Developments in Paleoenvironmental Research book series. The first volume (Last & Smol, 2001a) examined the acquisition and archiving of sediment cores, chronological techniques, and large-scale basin analysis methods. Volume 2 (Last & Smol, 2001b) focused on physical and chemical methods. Volume 3 (Smol et al. , 2001), along with this book, summarize the many biological methods and techniques that are available to study long-term environmental changeusing information preserved in sedimentary profiles. A subsequent volume (Birks et al. , in preparation) will deal with statistical and data handling procedures. It is our intent that these books will provide sufficient detail and breadth to be useful handbooks for both seasoned practitioners as well as newcomers to the area of paleolimnology. These books will also hopefully be useful to non-paleolimnologists (e. g. , limnologists, archeologists, palynologists, geographers, geologists, etc. ) who continue to hear and read about pal- limnology, but have little chance to explore the vast and sometimes difficult to access journal-based reference material for this rapidly expanding field. Although the chapters in these volumes target mainly lacustrine settings, many of the techniques described can also be readily applied to fluvial, glacial, marine, estuarine, and peatland environments. This current volume focuses on zoological indicators preserved in lake sediments, whilst Volume 3 focused on terrestrial, algal, and siliceous indicators.

Numerical and statistical methods have rapidly become part of a palaeolimnologist’s tool-kit. They are used to explore and summarise complex data, reconstruct past environmental variables from fossil assemblages, and test competing hypotheses about the causes of observed changes in lake biota through history. This book brings together a wide array of numerical and statistical techniques currently available for use in palaeolimnology and other branches of palaeoecology. ​ Visit http://extras.springer.com the Springer's Extras website to view data-sets, figures, software, and R scripts used or mentioned in this book.

Origins of fallout radionuclides Sediment records of fallout radionuclides Simple dating models Vertical mixing Numerical techniques Radiometric techniques Discussion Summary Acknowledgements References 10. chronostratigraphic techniques in paleolimnology. Svante Björck & Barbara Wohlfarth 205 Introduction Methods and problems Radiocarbon-dating different fractions of the sediment as a chronostratigraphic tool Dating of long (old) stratigraphies High resolution dating and wiggle matching dating versus absolute dating techniques of lacustrine sediments Concluding remarks Summary Useful www addresses Acknowledgements References 11. Varve chronology techniques. Scott Lamoureux 247 Introduction Methods Summary and future directions Acknowledgements References 12. Luminescence dating. Olav B. Lian & D.J. Huntley 261 Introduction The mechanism responsible for luminescence Dating and estimation of the paleodose Thermoluminescence dating Optical dating Evaluating the environmental dose rate xi Sample collection and preparation What types of depositional environments are suitable for luminescence dating? What can lead to an inaccurate optical age? Summary Acknowledgements References 13. Electron spin resonance (ESR) dating in lacustrine environments. Bonnie A.B. Blackwell 283 Introduction Principles of ESR analysis Sample collection ESR analysis ESR microscopy and other new techniques Applications and datable materials in limnological settings Summary Acknowledgements References 14. Use of paleomagnetism in studies of lake sediments. John King & John Peck 371 Introduction Recording fidelity of geomagnetic behavior by sediments Field and laboratory methods Holocene SV records Magnetostratigraphic studies of Neogene lake sediments Excursions, short events and relative paleointensity Conclusions Summary References 15. Amino acid racemization (AAR) dating and analysis in lacustrine environments.

This book, entitled Tracking Environmental Change Using Lake Sediments: Volume 6 – Sedimentary DNA, provides an overview of the applications of sedimentary DNA-based approaches to paleolimnological studies. These approaches have shown considerable potential in providing information about the long-term changes of overall biodiversity in lakes and their watersheds in response to natural and anthropogenic changes, as well as tracking human migrations over the last thousands of years. Although the first studies investigating the preservation of these molecular proxies in sediments originate from the late-1990s, the number of scientific publications on this topic has increased greatly over the last five years. Alongside numerous ecological findings, several sedimentary DNA studies have been dedicated to understanding the reliability of this approach to reconstruct past ecosystem changes. Despite the major surge of interest, a comprehensive compilation of sedimentary DNA approaches and applications has yet to be attempted. The overall aim of this DPER volume is to fill this knowledge gap.