Dedicated specifically to nuclear analytical techniques, this publication is intended to assist scientists using alpha, beta and gamma spectrometries, neutron activation and XRF analyses, and other nuclear analytical methods, in assessing and quantifying the sources of uncertainty in their daily measurements.

The purpose of this book is to present a state of art summary of current knowledge of methods of assessment of radionuclides in the terrestrial and marine environments. It cover the traditional methods of radioactivity measurements such as radiometrics techniques, but also recent developments in the mass spectrometry sector. The book starts with a short preface introducing the subject of the book, summarising content and philosophy of the book, as well as the most important historical achievements. The scientific topics are introduced by description of sampling methods, optimisation of sampling sites and sampling frequency. The recent developments in radiochemical separation methods using chromatography resins for the treatment of actinides, transuranics and other groups of radioelements are also described. No other book is available covering all aspects of environmental radioactivity measurements, although remarkable progress has been made in detection techniques over the last ten years. At present the new methods enable to carry out investigations which were not possible before, either because of lack of sensitivity or because of the fact that they required too large samples.

Authoritative reference providing the principles, practical techniques, and procedures for the accurate measurement of radioactivity.

Modern applications of nuclear chemistry concern various scientific disciplines, such as high-sensitive, high-selective, and non-destructive analytical technologies, pharmaceutical and medical research, molecular diagnosis and patient treatment, and nuclear energy. This book also discusses the issues waste managements and environmental aspects. The new edition has updated literature references and includes new material throughout.

Reliable and metrologically comparable results of quantitative analytical methods are essential to assure that decisions taken on their basis have meaning and context. Problems with combining measurement results, calculating their uncertainties and establishing metrological traceability can prove complicated and ambiguous for measurement scientists. Combining and Reporting Analytical Results discusses in detail the problems faced by scientists, and presents a variety of approaches across biological, chemical and environmental sciences to resolving these types of issues. Topics include: validated methods of analysis; application of internal quality control procedures; participation in proficiency testing schemes; metrological traceability of measurement results and associated uncertainties, as well as some quality system issues and formal accreditation. Written by leading experts, and with worked examples and illustrations throughout, this invaluable reference source is ideal for analysts from various scientific fields.

Chemical Analysis of Food: Techniques and Applications reviews new technology and challenges in food analysis from multiple perspectives: a review of novel technologies being used in food analysis, an in-depth analysis of several specific approaches, and an examination of the most innovative applications and future trends. This book won a 2012 PROSE Award Honorable Mention in Chemistry and Physics from the Association of American Publishers. The book is structured in two parts: the first describes the role of the latest developments in analytical and bio-analytical techniques and the second reviews the most innovative applications and issues in food analysis. Each chapter is written by experts on the subject and is extensively referenced in order to serve as an effective resource for more detailed information. The techniques discussed range from the non-invasive and non-destructive, such as infrared spectroscopy and ultrasound, to emerging areas such as nanotechnology, biosensors and electronic noses and tongues. Important tools for problem-solving in chemical and biological analysis are discussed in detail. - Winner of a PROSE Award 2012, Book: Honorable Mention in Physical Sciences and Mathematics - Chemistry and Physics from the American Association of Publishers - Provides researchers with a single source for up-to-date information in food analysis - Single go-to reference for emerging techniques and technologies - Over 20 renowned international contributors - Broad coverage of many important techniques makes this reference useful for a range of food scientists

The scienti c method is based on the measurement of di erent physical qu- tities and the search for relations between their values. All measured values of physical quantities are, however, a ected by uncertainty. Understanding the origin of uncertainty, evaluating its extent, and suitably taking it into account in data analysis, are fundamental steps for assessing the global accuracy of physical laws and the degree of reliability of their technological applications. The introduction to uncertainty evaluation and data analysis procedures is generally made in laboratory courses for freshmen. During my long-lasting teaching experience, I had the feeling of some sort of gap between the ava- able tutorial textbooks, and the specialized monographs. The present work aims at lling this gap, and has been tested and modi ed through a feedback interaction with my students for several years. I have tried to maintain as much as possible a tutorial approach, that, starting from a phenomenolo- cal introduction, progressively leads to an accurate de nition of uncertainty and to some of the most common procedures of data analysis, facilitating the access to advanced monographs. This book is mainly addressed to - dergraduate students, but can be a useful reference for researchers and for secondary school teachers. The book is divided into three parts and a series of appendices. Part I is devoted to a phenomenological introduction to measurement and uncertainty. In Chap.

Analytical chemical results touch everyones lives can we eat the food? do I have a disease? did the defendant leave his DNA at the crime scene? should I invest in that gold mine? When a chemist measures something how do we know that the result is appropriate? What is fit for purpose in the context of analytical chemistry? Many manufacturing and service companies have embraced traditional statistical approaches to quality assurance, and these have been adopted by analytical chemistry laboratories. However the right chemical answer is never known, so there is not a direct parallel with the manufacture of ball bearings which can be measured and assessed. The customer of the analytical services relies on the quality assurance and quality control procedures adopted by the laboratory. It is the totality of the QA effort, perhaps first brought together in this text, that gives the customer confidence in the result. QA in the Analytical Chemistry Laboratory takes the reader through all aspects of QA, from the statistical basics and quality control tools to becoming accredited to international standards. The latest understanding of concepts such as measurement uncertainty and metrological traceability are explained for a working chemist or her client. How to design experiments to optimize an analytical process is included, together with the necessary statistics to analyze the results. All numerical manipulation and examples are given as Microsoft Excel spreadsheets that can be implemented on any personal computer. Different kinds of interlaboratory studies are explained, and how a laboratory is judged in proficiency testing schemes is described. Accreditation to ISO 17025 or OECD GLP is nearly obligatory for laboratories of any pretension to quality. Here the reader will find an introduction to the requirements and philosophy of accreditation. Whether completing a degree course in chemistry or working in a busy analytical laboratory, this book is a single source for an introduction into quality assurance.

The Oxford Handbook of Nuclear Security provides a comprehensive examination of efforts to secure sensitive nuclear assets and mitigate the risk of nuclear terrorism and other non-state actor threats. It aims to provide the reader with a holistic understanding of nuclear security through exploring its legal, political, and technical dimensions at the international, national, and organizational levels. Recognizing there is no one-size-fits-all approach to nuclear security, the book explores fundamental elements and concepts in practice through a number of case studies which showcase how and why national and organizational approaches have diverged. Although focused on critiquing past and current activities, unexplored yet crucial aspects of nuclear security are also considered, and how gaps in international efforts might be filled. Contributors to the handbook are drawn from a variety of different disciplinary backgrounds and experiences, to provide a wide range of perspectives on nuclear security issues and move beyond the Western narratives that have tended to dominate the debate.These include scholars from both developed and developing nuclear countries, as well as practitioners working in the field of nuclear security in an effort to bridge the gap between theory and practice.