The aim of this book is to familiarize the reader with the practical aspects of polymer analysis. A wealth of practical detail, including some detailed methods is included. The book covers not only the analysis of the main types of polymers and copolymers now in use commercially, but also the analysis of minor non-polymeric components of the polymer formulation, whether they be deliberately added, such as processing additives, or whether they occur adventitiously, such as moisture and residual monomers and solvent. A broad scheme for the examination of polymers is discussed in Chapter 2. Practically all of the major newer analytical techniques and many of the older classical techniques, have been used to examine polymers and their additive systems. As so many different polymers are now used commercially it is also advisable when attempting to identify a polymer to classify it by first separating it into pure polymeric and gross non polymeric fractions (Chapter Z) and then carrying out at least a qualitative elemental analysis and possible a quantitative analysis (Chapters 3 and 4) and then in some cases, depending on the elements found, to carry out functional group analysis (Chapters 6 and 9).

This book introduces the techniques used for the analysis of polymers. It covers the main aspects of polymer science and technology; identification, polymerization, molecular weight, structure, surface properties, degradation and mechanical properties. * Clear explanations of each analytical technique * Describes the application of techniques to the study of polymers * Encourages learning through numerous self-assessment questions and answers * Structured for flexible learning

Ein Praxisleitfaden der Polymeranalyse für alle, die sich in Polymerlabors mit Analytik, Qualitätskontrolle oder Produktentwicklung beschäftigen. Der Autor erläutert, aus seinem umfangreichen Erfahrungsschatz, welche Probleme in welchen Situationen auftreten können. Viele Fallstudien helfen bei der Anwendung der Erkenntnisse im Laboralltag. Mit einer umfangreichen Datensammlung zu physikalischen Eigenschaften von Polymeren! (07/00)

Analysis of Flame Retardancy in Polymer Science is a scientific/practical book that is conceptualized, designed, and written for students, early-career researchers, and junior engineers to explain the basic principles of fire analysis/characterization methods/methodologies, from flammability, ignition, and fire spread to forced convection and related analyses and to elucidate the mechanisms underlying flame retardancy in both gas and condensed phases followed by correlation between laboratory- and real-scale fire analyses as well as fire analysis from an industrial standpoint. This book is also an indispensable resource for identifying and mounting the latest achievements in fire analysis/characterization methods to frame the effects of fire evaluation strategies to be utilized for research and development. The book also gives a broad description of fire analysis related to different standards and regulations for different applications in different geographic zones. - Includes the background, fundamental, and modern features of techniques of characterization of fire and flame behavior - Provides an overview of the major techniques used in fire analysis of flame-retardant polymers - Characterizes different types of materials at small, bench, and real-life scale - Offers a comprehensive overview of fire behavior and testing and associated toxicity issues - Integrates the scientific, technical, standard, regulation, and industrial aspects of fire analysis into a book for future developments in the field

This laboratory manual covers important techniques for polymer synthesis and characterization, and provides newcomers with a comprehensive introduction to the basic principles of highlighted techniques. The reader will benefit from the clear writing style and straightforward approach to fairly complex ideas. The book also provides references that the more advanced reader can use to obtain in-depth explanations of techniques. Polymer Synthesis and Characterization will serve as a useful resource for industrial technicians and researchers in polymer chemistry and physics, material science, and analytical chemistry. - Combines the extensive industrial and teaching experience of the authors - Introduces the user to the concept of "Good Manufacturing Practice" - Presents experiments that are representative of a wide variety of polymerization and characterization methods - Includes numerous references for more advanced students, technicians, and researcher

This book is a practical manual for those who analyze polymers. Self-contained chapters describe when a technique should be selected, explain its basic principles, describe how instruments are constructed and operated, and teach how the data obtained relate to molecular structure and physical properties. Many clear illustrations are included. Implicit memory refers to a change in task performance due to an earlier experience that is not consciously remembered. This book is not a research manual but rather a guide to performing and understanding polymer characterization and an introduction to the specialized literature of the analytical chemistry of polymers. The techniques covered are directly relevant to the characterization of synthetic polymers such as adhesives, sealants, polymers, composites, coatings, elastomers, rubber, and other nonmetallic materials. Many techniques are also quite useful for natural and biological polymers.

Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.

Based on Wiley's renowned Encyclopedia of Polymer Science and Technology, this book provides coverage of key methods of characterization of the physical and chemical properties of polymers, including atomic force microscopy, chromatographic methods, laser light scattering, nuclear magnetic resonance, and thermal analysis, among others. Written by prominent scholars from around the world, this reference presents over twenty-five self -contained articles on the most used analytical techniques currently practiced in polymer science.

Designed to provide both an introduction and a practical guide to all aspects of polymer analysis, this book covers not only the various types of polymer now in commercial use, but also the minor non-polymeric components of their formulation, whether added deliberately, for example to improve service life, or present through the action of adventitious moisture, unreacted monomer, or excess solvent. All analytical techniques have been included, from the older, classical techniques of both elemental and functional group analysis, to the most modern physical techniques, including the various types of spectroscopy, gas chromatography-mass spectrometry, ozoneolysis, thermal methods, fractionation, and electron probe microanalysis. In each case, the technique is explained in detail, allowing the analyst to develop the considerable range of skills required to provide as complete a picture as possible of the polymer's structure. The extensive use of tables, the inclusion of numerous spectra and chemical formulae, and a comprehensive reference list ensure that this book will be of lasting use, for both the student and the practising analytical chemist.

MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.