Multidimensional Analytical Techniques in Environmental Research is a comprehensive resource on the many multidimensional analytical strategies to qualitatively and quantitatively assess and map the organic and inorganic pollutants in complex atmospheric, water and soil matrices. During the past two decades, the rapidly-evolving field of analytical instrumentation has produced sophisticated multidimensional tools capable of providing unique and in-depth knowledge on the chemical features of complex mixtures from these different environmental matrices. This book brings together the wealth of information in the current literature, assisting in the decision-making process by covering both the fundamentals and applications of these methodologies. Sections cover the wide variety of multidimensional analytical techniques, including multidimensional solution- and solid-state nuclear magnetic resonance (NMR) spectroscopy, ultrahigh-resolution mass spectrometry (MS), two-dimensional correlation spectroscopy, two-dimensional liquid and gas chromatography and capillary electrophoresis coupled to high-resolution detection techniques, and excitation-emission (EEM) fluorescence spectroscopy assisted by multiway data analysis tools, and the use of synchrotron-radiation-based techniques combined with other spectroscopic approaches to explore and map the speciation of elements. - Identifies state-of-the-art multidimensional analytical methods for targeted and untargeted profiling of complex mixtures from different environmental matrices (soil, sediment, water, and air) - Assesses the advantages and limitations of the most modern and sophisticated multidimensional analytical methods in environmental research - Highlights the current challenges and potential future directions in the application of multidimensional analytical tools to advance the current understanding on the dynamics and fate of environmental pollutants in different environmental matrices

La diversidad biológica es fruto de la interacción entre numerosas especies, ya sean marinas, vegetales o animales, a la par que de los muchos factores limitantes que caracterizan el medio que habitan. El análisis multivariante utiliza las relaciones entre diferentes variables para ordenar los objetos de estudio según sus propiedades colectivas y luego clasificarlos; es decir, agrupar especies o ecosistemas en distintas clases compuestas cada una por entidades con propiedades parecidas. El fin último es relacionar la variabilidad biológica observada con las correspondientes características medioambientales. Multivariate Analysis of Ecological Data explica de manera completa y estructurada cómo analizar e interpretar los datos ecológicos observados sobre múltiples variables, tanto biológicos como medioambientales. Tras una introducción general a los datos ecológicos multivariantes y la metodología estadística, se abordan en capítulos específicos, métodos como aglomeración (clustering), regresión, biplots, escalado multidimensional, análisis de correspondencias (simple y canónico) y análisis log-ratio, con atención también a sus problemas de modelado y aspectos inferenciales. El libro plantea una serie de aplicaciones a datos reales derivados de investigaciones ecológicas, además de dos casos detallados que llevan al lector a apreciar los retos de análisis, interpretación y comunicación inherentes a los estudios a gran escala y los diseños complejos.

The environment is considered the surroundings in which an organism operates, including air, water, land, natural resources, flora, fauna, humans and their interrelation. It is this environment which is both so valuable, on the one hand, and so endangered on the other. And it is people who are by and large ruining the environment both for themselves and for all other organisms. This book reviews the latest research in this field which is vital for everyone.

Environmental Metabolomics Applications in Field and Laboratory Studies: From the Exposome to the Metabolome presents an overview of the current state of aquatic environments and problems caused by human pressure and daily life. The presence of contaminants in nature and their effects are evaluated, along with recommendations for preservation. This book not only shows readers how to implement techniques, it also guides them through the process. As metabolomics becomes a more routine technique for environmental studies and future perspectives, a guide for validation and globalization of current approaches is needed.

Global climate change is the most important challenge humankind is facing in the modern era. One of the main scientific concerns is the monitoring of contaminants in the environment, which require the right environmental remediation strategies. In this context, nuclear magnetic resonance (NMR) techniques have a very important role in enabling the discovery of how pollutants are transformed, how they can move and how they can affect human health. This book discusses the present and the future perspectives of NMR techniques for environmental evaluations. It covers, amongst other topics, the importance of NMR as a contamination discovery tool, how to improve sensitivity in environmental NMR, and multiphase NMR for measurement of samples in their natural state. Samples include lubricant oils, soils and porous media. Due to the direct relationship between the environment and human health, there is information dedicated to the use of magnetic resonance imaging (MRI) to monitor human health as related to environmental pollution. There is also a chapter on how NMR is used in cultural heritage to measure artefacts directly affected by environmental pollution. Filling a gap in the literature, the book is for researchers explaining how to apply their knowledge of NMR techniques to solve environmental problems, and for students who want to deepen their understanding of this topic.

The book explains the principles and fundamentals of Green Analytical Chemistry (GAC) and highlights the current developments and future potential of the analytical green chemistry-oriented applications of various solutions. The book consists of sixteen chapters, including the history and milestones of GAC; issues related to teaching of green analytical chemistry and greening the university laboratories; evaluation of impact of analytical activities on the environmental and human health, direct techniques of detection, identification and determination of trace constituents; new achievements in the field of extraction of trace analytes from samples characterized by complex composition of the matrix; “green” nature of the derivatization process in analytical chemistry; passive techniques of sampling of analytes; green sorption materials used in analytical procedures; new types of solvents in the field of analytical chemistry. In addition green chromatography and related techniques, fast tests for assessment of the wide spectrum of pollutants in the different types of the medium, remote monitoring of environmental pollutants, qualitative and comparative evaluation, quantitative assessment, and future trends and perspectives are discussed. This book appeals to a wide readership of the academic and industrial researchers. In addition, it can be used in the classroom for undergraduate and graduate Ph.D. students focusing on elaboration of new analytical procedures for organic and inorganic compounds determination in different kinds of samples characterized by complex matrices composition.Jacek Namieśnik was a Professor at the Department of Analytical Chemistry, Gdańsk University of Technology, Poland. Justyna Płotka-Wasylka is a teacher and researcher at the same department.

Organic contaminants even in very low concentrations can have toxic and ecotoxic effects on exposed organisms. Detection and quantification of such trace amounts in diverging matrices (e.g., water, air, soil, food, tissue, organisms) is challenging and great carefulness and strategic thinking is needed to get reliable results along the way from taking samples up to the final analysis. In the 2nd edition, besides revisions of existing chapters, new analytical technologies and recent application examples are presented: non-target mass spectrometric analysis, trace analysis of per- and polyfluoroalkylated "forever chemicals", organophosphorus esters (nerve agents), and micro- and nanoplastic particles in the environment. Students will learn about peculiarities and state of the art organic trace analysis and acquire basic and advanced principles of statistical evaluation of analytical results quality control strategies and good laboratory practices sampling techniques from various matrices sample treatment, enrichment and clean-up techniques chromatographic analyses including hyphenated techniques, and spectroscopy as well mass spectrometry and bioanalytical tools. An extended chapter on selected applications will transfer the theoretical understanding into applied scientific problems. Students will profit from a comprehensive and state of the art overview of organic trace analyses and from an extensive collection of relevant literature.

"In full colour throughout, this book describes the power of mass spectrometry in resolving environmental issues, demonstrating how real-world complex problems can be solved in a simple and elegant way."--Worldcat.

When the Cold War abruptly ended, DOE halted most nuclear materials production. In 1995, Congress chartered DOE's Environmental Management Science Program (EMSP) to bring the nation's scientific infrastructure to bear on EM's most difficult, long-term cleanup challenges. The EMSP provides grants to investigators in industry, national laboratories, and universities to undertake research that may help address these cleanup challenges. On several occasions the EMSP has asked the National Academies for advice on developing its research agenda. This report resulted from a 15-month study by an Academies committee on long-term research needs for deactivation and decommissioning (D&D) at DOE sites.