A comprehensive treatment of the subject of microscale inorganic chemistry is provided through 45 laboratory experiments. These include experiments in main group and transition metal chemistry, instrumental techniques, kinetics, synthesis and the manipulation of air-sensitive material.

"Compatible with standard taper miniscale, 14/10 standard taper microscale, Williamson microscale. Supports guided inquiry"--Cover.

Previously by Angelici, this laboratory manual for an upper-level undergraduate or graduate course in inorganic synthesis has for many years been the standard in the field. In this newly revised third edition, the manual has been extensively updated to reflect new developments in inorganic chemistry. Twenty-three experiments are divided into five sections: solid state chemistry, main group chemistry, coordination chemistry, organometallic chemistry, and bioinorganic chemistry. The included experiments are safe, have been thoroughly tested to ensure reproducibility, are illustrative of modern issues in inorganic chemistry, and are capable of being performed in one or two laboratory periods of three or four hours. Because facilities vary from school to school, the authors have included a broad range of experiments to help provide a meaningful course in almost any academic setting. Each clearly written & illustrated experiment begins with an introduction that hig! hlights the theme of the experiment, often including a discussion of a particular characterization method that will be used, followed by the experimental procedure, a set of problems, a listing of suggested Independent Studies, and literature references.

Inorganic chemistry is the study of all chemical compounds except those containing carbon, which is the field of organic chemistry. There is some overlap since both inorganic and organic chemists traditionally study organometallic compounds. Inorganic chemistry has very important ramifications for industry. Current research interests in inorganic chemistry include the discovery of new catalysts, superconductors, and drugs to combat disease. This new volume covers a diverse collection of topics in the field, including new methods to detect unlabeled particles, measurement studies, and more.

In the past two decades, microscale techniques have soared in popularity because these techniques minimize exposure to potentially dangerous chemicals in the lab, drastically cut the amount of chemical waste, lower costs, and reduce risks of chemical fires and explosions. The result is a safer and healthier laboratory environment. Now, with Microscale General Chemistry Laboratory with Selected Macroscale Experiments, Second Edition, you can bring these techniques into your own chemistry lab. Thoroughly revised with updated experiments, the new Second Edition continues to offer a large variety of well-designed, easy-to-follow experiments, as well as thorough background information and an outstanding selection of questions and problems.

Featuring new experiments unique to this lab textbook, as well as new and revised essays and updated techniques, this Sixth Edition provides the up-to-date coverage students need to succeed in their coursework and future careers. From biofuels, green chemistry, and nanotechnology, the book’s experiments, designed to utilize microscale glassware and equipment, demonstrate the relationship between organic chemistry and everyday life, with project-and biological or health science focused experiments. As they move through the book, students will experience traditional organic reactions and syntheses, the isolation of natural products, and molecular modeling. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.

For more than a quarter century, Cotton and Wilkinson's Advanced Inorganic Chemistry has been the source that students and professional chemists have turned to for the background needed to understand current research literature in inorganic chemistry and aspects of organometallic chemistry. Like its predecessors, this updated Sixth Edition is organized around the periodic table of elements and provides a systematic treatment of the chemistry of all chemical elements and their compounds. It incorporates important recent developments with an emphasis on advances in the interpretation of structure, bonding, and reactivity.“/p> From the reviews of the Fifth Edition: "The first place to go when seeking general information about the chemistry of a particular element, especially when up-to-date, authoritative information is desired." —Journal of the American Chemical Society "Every student with a serious interest in inorganic chemistry should have [this book]." —Journal of Chemical Education "A mine of information . . . an invaluable guide." —Nature "The standard by which all other inorganic chemistry books are judged." —Nouveau Journal de Chimie "A masterly overview of the chemistry of the elements." —The Times of London Higher Education Supplement "A bonanza of information on important results and developments which could otherwise easily be overlooked in the general deluge of publications." —Angewandte Chemie

This updated revision offers total coverage of organic laboratory experiments and techniques focusing on modern laboratory instrumentation, a strong emphasis on lab safety, additional concentration on sequential reaction sequences, excellent pre- and post-lab exercises, and multistep experiments which maximize the number of manipulations students perform per lab period. The microscale approach is low in cost, offers ease of doing experiments and uses minimal amounts of chemicals. A number of experiments include instructions for scaling up.

This laboratory manual utilizes an investigative approach which departs from the traditional format of providing experiments with predetermined solutions. Includes both microscale and macroscale experiments which cover topics such as biochemistry, polymer chemistry and materials science.