Cutting edge high temperature materials include high temperature superconductors, solid oxide fuel cells, thermoelectric materials and ultrahigh temperature construction materials (including metals, cermets and ceramics) and have applications in key areas such as energy, transportation and space technologies. This book introduces the concepts which underpin research into these critical materials including thermodynamics, kinetics and various physical, chemical and modelling techniques with a focus on practical “how to” methods and covers: Introduction to High Temperature Research Basic Design of High Temperature Furnaces Temperature Measurement Radiation Pyrometry Refractory Materials in the Laboratory Vacuum in Theory and Practice The Design of Vacuum Furnaces and Thermobalances With highly detailed instrument illustrations and an emphasis on the control and measurement of the fundamental properties of temperature, pressure and mass, High Temperature Experiments in Chemistry and Materials Science provides a practical reference on high temperature measurements, for researchers, advanced students and those working in academic or industrial laboratories. Introduction to High Temperature Research Basic Design of High Temperature Furnaces Temperature Measurement Radiation Pyrometry Refractory Materials in the Laboratory Vacuum in Theory and Practice The Design of Vacuum Furnaces and Thermobalances

This book presents a summary of high-pressure phase transitions of minerals and related inorganic compounds. The first part reviews the methods to investigate phase transitions by direct high-pressure and high-temperature experiments together with thermodynamic approaches that consist of calorimetric measurements and thermodynamic calculation. In the second part, phase relations and thermodynamic properties of olivine, pyroxene, garnet, spinel, perovskite, rutile, and related inorganic compounds with A2BO4, ABO3, AB2O4, and AO2 stoichiometries are described. Particular emphasis is placed on spinel- and perovskite-structured phases and their high-pressure polymorphs called post-spinel and post-perovskite phases. The last part of the book focuses on phase relations of mantle rocks and on natural high-pressure minerals from the Earth’s deep mantle and in shocked meteorites.

This English translation of a well-known Japanese book covers interfacial physicochemistry in materials science, especially for iron- and steelmaking processes. Interfacial Physical Chemistry of High-Temperature Melts bridges the gap between the basics and applications of physicochemistry. The book begins with an overview of the fundamentals of interfacial physical chemistry and discusses surface tension, describing the derivation of important equations to guide readers to a deep understanding of the phenomenon. The book then goes on to introduce interfacial properties of high-temperature melts, especially the Marangoni effect, and discusses applications to materials processing at high temperature focusing on recent research results by the author and the co-workers. This book is aimed at researchers, graduate students, and professionals in materials processing. Video clips of in-situ observation including experiments under microgravity condition and x-ray observation are available for download on the publisher's website to allow for a deeper understanding.

This compendium of twenty laboratory experiments on metals and alloys attempts to provide to students of Science and Engineering an insight about the relationship of the physical, specially mechanical properties of metals with grain structures/microstructures. In almost all the experiments, therefore, the microstructural investigation is provided. Experiments have also been included on the determination of important mechanical and thermal properties and on the aqueous and atmospheric corrosion of metals. Theoretical background of each experiment has been dealt with in good detail in order to enable the student to understand the underlying principles and to appreciate the significance of the experiments. Information which could not be accommodated given in the text of the experiments, has been provided in the form of appendices.These include: reflection microscopy, experimental determination of transition points through cooling curves to get data for plotting phase diagrams, and quenching media for tempering of alloys. In view of the importance of microstrucures for some metals and alloys have also been given.

This first volume provides the basic matters needed for understanding the thermophysical properties of metallic liquids and for developing reliable models to accurately predict the thermophysical properties of almost all metallic elements in the liquid state, together with methods for quantitative assessment of models/equations. The authors also review the structure of metallic liquids, which is based on the theory of liquids, density, volume expansivity, thermodynamic properties (evaporation enthalpy, vapour pressure, heat capacity), sound velocity, surface tension, viscosity, diffusion, and electrical and thermal conductivities. Finally, the essential points of methods used for measuring these experimental data are presented.

This title analyzes the chemical reactions, structures and fundamental properties of supercritical fluid systems for the production of new compounds, nanomaterials, fibers, and films. It compiles contemporary research and technological advances for increased selectivity and reduced waste in chemical, industrial, pharmaceutical, and biomedical applications. Topics include fluid dynamics, catalysis, hydrothermal synthesis, surfactants, conducting polymers, crystal growth, and other aspects and applications of supercritical fluids.